STRUCTURAL BASIS OF DNA FOLDING AND RECOGNITION IN AMP-DNA APTAMER COMPLEX, NMR, 7 STRUCTURES
SOLUTION NMR
NMR Experiment | ||||||||
---|---|---|---|---|---|---|---|---|
Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
1 | NOESY | 6.35 | 278 | |||||
2 | TOCSY | 6.35 | 278 | |||||
3 | COSY | 6.35 | 278 | |||||
4 | 1H-13C HMQC | 6.35 | 278 |
NMR Spectrometer Information | |||
---|---|---|---|
Spectrometer | Manufacturer | Model | Field Strength |
1 | Varian | VARIAN INOVA 600 | 600 |
NMR Refinement | ||
---|---|---|
Method | Details | Software |
DISTANCE GEOMETRY AND DISTANCE RESTRAINED MD | REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVE. | X-PLOR |
NMR Ensemble Information | |
---|---|
Conformer Selection Criteria | LEAST TOTAL ENERGY, NOE VIOLATION, VDW |
Conformers Calculated Total Number | 21 |
Conformers Submitted Total Number | 7 |
Computation: NMR Software | ||||
---|---|---|---|---|
# | Classification | Version | Software Name | Author |
1 | refinement | X-PLOR | 3.1 | BRUNGER |
2 | structure solution | XVNMR | ||
3 | structure solution | X-PLOR |